Preparation and Application of (GMA-co-ACA co-AAM) as Cation-Exchange Monolithic Column for determination Nickel (II) ion

Authors

  • Salam M. Nasser

Keywords:

GMA, Monolith, Ion exchange column, Nickel (II) .

Abstract

Ion exchange chromatography was created using a polymer-based monolithic column as a strong cation-exchange column with various
function groups. Acrylic acid (A. acid), glycidyl methacrylate (GMA), and acryl amid were used to make monolithic columns via free radical
polymerization (A. amid). The epoxy rings were then sulfonated at 70°C using Na2
SO3
. A model of common cation of Ni(II) spectrophotometry
was used to assess the monolithic column, which was compared to atomic absorption approach. The LOD and LOQ were 0.001 g/mL and 0.002
g/mL, respectively, while the linearity (R2) was 0.9980. FTIR, Brunauer-Emmett-Teller (BET) analysis, and scanning electron microscopy
were used to analyze the cation-exchange columns (SEM).

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Published

2022-06-30

Issue

Vol. 13 No. 2 (2022)

Section

Articles

How to Cite

Preparation and Application of (GMA-co-ACA co-AAM) as Cation-Exchange Monolithic Column for determination Nickel (II) ion. (2022). Journal of Pharmaceutical Negative Results, 13(2), 92-96. https://mail.pnrjournal.com/index.php/home/article/view/210